0.05),,此時(shí)液固比不再是影響攪拌轉(zhuǎn)速的主要因素,;當(dāng)液固比小于40 mL/g,、攪拌轉(zhuǎn)速大于150 r/min時(shí),,極板間距是影響物料升溫速率的主要因素,,隨著極板間距的減小,,升溫速率不斷加快,,當(dāng)極板間距為130 mm時(shí),,升溫速率可達(dá)到8~10℃/min,。"/>

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基于射頻波強(qiáng)化的試驗(yàn)型水熱反應(yīng)器研究
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陜西省重點(diǎn)研發(fā)計(jì)劃項(xiàng)目(2023YBNY150)


Design and Testing of Experimental Hydrothermal Reactor Based on Radio Frequency Intensification
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    摘要:

    針對水熱提取反應(yīng)目前主要依靠微波強(qiáng)化,存在穿透深度小,、加熱均勻性差的問題,,利用加熱均勻性更好的射頻波為熱源,基于常見的水平式平行極板射頻加熱系統(tǒng)設(shè)計(jì)了一套適用于射頻強(qiáng)化的水熱反應(yīng)器,。該水熱反應(yīng)器主要由雙層反應(yīng)釜,、壓力調(diào)節(jié)裝置、光纖測溫計(jì)和氣動(dòng)磁力攪拌器4部分構(gòu)成,,首先對整機(jī)結(jié)構(gòu)及工作原理進(jìn)行闡述,,然后基于內(nèi)壓薄壁圓筒應(yīng)力分析理論和磁力耦合傳動(dòng)理論對雙層反應(yīng)釜和氣動(dòng)磁力攪拌器的關(guān)鍵零部件進(jìn)行設(shè)計(jì),并完成了壓力調(diào)節(jié)裝置和測溫方式的設(shè)計(jì)和選型,,最后完成射頻強(qiáng)化水熱反應(yīng)試驗(yàn)平臺的搭建,,并選取攪拌轉(zhuǎn)速、液固比和射頻極板間距對水熱反應(yīng)器的攪拌和升溫性能進(jìn)行了測試,。結(jié)果表明:當(dāng)液固比大于20 mL/g時(shí),,攪拌轉(zhuǎn)速與對照樣品純水無顯著差異(p>0.05),此時(shí)液固比不再是影響攪拌轉(zhuǎn)速的主要因素,;當(dāng)液固比小于40 mL/g,、攪拌轉(zhuǎn)速大于150 r/min時(shí),,極板間距是影響物料升溫速率的主要因素,隨著極板間距的減小,,升溫速率不斷加快,,當(dāng)極板間距為130 mm時(shí),升溫速率可達(dá)到8~10℃/min,。

    Abstract:

    Since the current researches about hydrothermal extraction was mainly relying on microwave intensification, which has the problems of small penetration depth and poor heating uniformity, a method of radio frequency (RF) with better heating uniformity was used to heat and a set of hydrothermal reactor suitable for RF intensification was designed based on the horizontal parallel electrodes RF heating system. This hydrothermal reactor was mainly composed of four parts: double-layer autoclave, pressure regulator, fiber-optical thermometer and air-driven magnetic stirrer. Firstly, the overall structure and working principle were explained. Then the key components of the double-layer autoclave and air-driven magnetic stirrer were designed in detail based on the stress analysis theory of the internal pressure thin-wall cylinder and the magnetic coupling transmission theory, and the pressure regulator and fiber-optical thermometer were designed and selected, respectively. Finally, the experimental platform of RF intensify hydrothermal reaction was built and the stirring speed, liquid/solid ratio (LSR) and RF electrode gap were selected to test the stirring and heating performance of the hydrothermal reactor. The results showed that there was no significant difference for the stirring speed between the experimental groups and control group (pure water), when the LSR was greater than 20 mL/g (p>0.05), and the LSR was no longer the main factor affecting the stirring speed. When the LSR was less than 40 mL/g, and the stirring speed was greater than 150 r/min, the electrodes gaps was the main factor affecting the heating rate of sample, and the heating rate was increased continuously with the reduction of the electrodes gaps. When the electrodes gap was 130 mm, the heating rate can reach 8~10℃/min. The development of this reactor can provide important technical support for the experimental research of hydrothermal extraction based on RF intensification.

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仵明太,張浩,張一鳴,段鈺婷,王博文,王紹金,令博.基于射頻波強(qiáng)化的試驗(yàn)型水熱反應(yīng)器研究[J].農(nóng)業(yè)機(jī)械學(xué)報(bào),2024,55(9):450-458. WU Mingtai, ZHANG Hao, ZHANG Yiming, DUAN Yuting, WANG Bowen, WANG Shaojin, LING Bo. Design and Testing of Experimental Hydrothermal Reactor Based on Radio Frequency Intensification[J]. Transactions of the Chinese Society for Agricultural Machinery,2024,55(9):450-458.

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  • 收稿日期:2024-05-06
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  • 在線發(fā)布日期: 2024-09-10
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