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China is the biggest concentrated apple juice producer in the world with a production of millions of tons of apple pomace every year. It is an important comprehensive utilizing approach by separating of polyphenols from apple pomace. A nano-material for adsorption of polyphenols from apple pomace was prepared. The moulding condition and preparation process of methylacrylic acid nano-materials was optimized by changing the dosage of methylacrylic acid(MAA), ethylene glycol dimethacrylate(EDMA), azodiisobutyronitrile(AIBN) and acetonitrile, using chemical precipitation method and field emission scanning electron microscopy, and conducting the experiments of adsorbing of polyphenols from apple pomace by the prepared nano-material, so as to provide reference for the comprehensive utilization of apple residue. The results showed that the best preparation condition of this material was methylacrylic acid of 2.5mmol, ethylene glycol dimethacrylate of 2.5mmol, azodiisobutyronitrile of 1.00mmol and acetonitrile of 20mL, under which the adsorption capacity of obtained nano-material to polyphenols could achieve to 33.42mg/g, and the desorption rate was 61.13% at the same time. 